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CNT-based MEMS/NEMS gas ionizers for portable mass spectrometry applications

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Velaasquez-2010-CNT-based MEMSNEMS gas ionizers for portable mass spectrometry applications.pdf

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Author(s)
Velasquez-Heller, Luis Fernand
•
Gassend, Blaise
•
Akinwande, Akintunde Ibitayo
Date Issued
June 2010
Journal
Journal of Microelectromechanical Systems
Publisher
Institute of Electrical and Electronics Engineers (IEEE)
Citation
Velasquez-Garcia, Luis Fernando, Blaise Laurent Patrick Gassend, and Akintunde Ibitayo Akinwande. “CNT-Based MEMS/NEMS Gas Ionizers for Portable Mass Spectrometry Applications.” Journal of Microelectromechanical Systems 19.3 (2010): 484–493. Web. 25 May 2012. © 2010 Institute of Electrical and Electronics Engineers
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Final published version
Abstract
We report the fabrication and experimental characterization of a carbon nanotube (CNT)-based MEMS/NEMS electron impact gas ionizer with an integrated extractor gate for portable mass spectrometry. The ionizer achieves low-voltage ionization using sparse forests of plasma-enhanced chemical-vapor-deposited CNTs as field emitters and a proximal extractor grid with apertures aligned to the CNT forests to facilitate electron transmission. The extractor gate is integrated to the ionizer using a high-voltage MEMS packaging technology based on Si springs defined by deep reactive ion etching. The ionizer also includes a high-aspect-ratio silicon structure (??foam) that facilitates sparse CNT growth and also enables uniform current emission. The devices were tested as field emitters in high vacuum (10[superscript -8] torr) and as electron impact ionizers using argon at pressures of up to 21 mtorr. The experimental data show that the MEMS extractor gate transmits up to 66% of the emitted current and that the ionizers are able to produce up to 0.139 mA of ion current with up to 19% ionization efficiency while consuming 0.39 W.
MIT Department
Massachusetts Institute of Technology. Department of Electrical Engineering and Computer Science
Massachusetts Institute of Technology. Microsystems Technology Laboratories
Terms of Use
Article is made available in accordance with the publisher's policy and may be subject to US copyright law. Please refer to the publisher's site for terms of use.
Persistent DSpace Link
http://hdl.handle.net/1721.1/70945
DOI of Published Version
https://doi.org/10.1109/JMEMS.2010.2045639
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