Rapid 3D MAS NMR Spectroscopy at Critical Sensitivity
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Matsuki_AC_49_1-5(2010).pdf
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Author(s)
Matsuki, Yoh
Eddy, Matthew Thomas
Griffin, Robert Guy
Herzfeld, Judith
Alternative Title
Rapid Three-Dimensional MAS NMR Spectroscopy at Critical Sensitivity
Date Issued
October 2010
Journal
Angewandte Chemie International Edition
Publisher
Wiley-Blackwell Pubishers
Citation
Matsuki, Yoh et al. “Rapid Three-Dimensional MAS NMR Spectroscopy at Critical Sensitivity.” Angewandte Chemie International Edition 49.48 (2010): 9215–9218. Web.
Version
Author's final manuscript
Abstract
Sensitive SIFTing: Multidimensional non-uniform sampling (NUS) NMR spectroscopy is extended to the severely sensitivity-limited regime typical of MAS NMR of biomacromolecules by the use of spectroscopy by the integration of frequency and time domain information (SIFT). A three-dimensional MAS NMR experiment is expedited (here 3.4-fold) without losing sensitivity or resolution.
MIT Department
Massachusetts Institute of Technology. Department of Chemistry
Francis Bitter Magnet Laboratory (Massachusetts Institute of Technology)
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Creative Commons Attribution-Noncommercial-Share Alike 3.0
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DOI of Published Version
https://doi.org/10.1002/anie.201003329
