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Heather Lechtman. Biçer, Katherine K. (Katherine Kershen) Massachusetts Institute of Technology. Dept. of Materials Science and Engineering. Massachusetts Institute of Technology. Department of Materials Science and Engineering 2006-07-13T15:20:58Z 2006-07-13T15:20:58Z 2005 2005 http://hdl.handle.net/1721.1/33398 62708458 Thesis (S.M.)--Massachusetts Institute of Technology, Dept. of Materials Science and Engineering, 2005. Includes bibliographical references (leaves 91-96). A three phase analytical protocol is developed to systematize the study of multifaceted serpentinite bronze-casting moulds from Bronze Age Anatolia (ca. 3500-1700 B.C.). These moulds represent a class of metal processing tools that reflect material properties and perhaps also social concerns in their development and use. In phase I of the protocol, standard serpentinite tiles are heated to known temperatures and the crack density and ineral changes at each temperature are determined using scanning electron microscopy (SEM) and energy dispersive x-ray (EDX) analysis. These results then serve to calibrate the cracking and mineralogical behaviors of serpentinite replica moulds used in controlled casting experiments during phase II. Metallography on several phase II cast objects provides additional information on heat flow through the stone. In phase III, the protocol is modified appropriately for the non-destructive study of four archaeological moulds using x-ray diffraction (XRD), x-ray fluorescence (XRF), and SEM. The applicability of the protocol to other stone and ceramic materials is discussed. by Katherine K. Biçer. S.M. 193 leaves 15895523 bytes 15903739 bytes application/pdf application/pdf eng Massachusetts Institute of Technology M.I.T. theses are protected by copyright. They may be viewed from this source for any purpose, but reproduction or distribution in any format is prohibited without written permission. See provided URL for inquiries about permission. http://dspace.mit.edu/handle/1721.1/7582 Materials Science and Engineering. Multifaced stone and ceramic moulds from Bronze Age Anatolia : building an analytical protocol of mould properties and behavior during the process of metal casting Thesis application/pdf false Publication unknown unknown <Publication xmlns="https://www.openaire.eu/cerif-profile/1.1/" id="f06750f1-6547-4e8a-bfa2-0cda1e8eda09"> <Type xmlns="https://www.openaire.eu/cerif-profile/vocab/COAR_Publication_Types">http://purl.org/coar/resource_type/c_1843</Type> <Language>eng</Language> <Title>Multifaced stone and ceramic moulds from Bronze Age Anatolia : building an analytical protocol of mould properties and behavior during the process of metal casting</Title> <PublishedIn> <Publication> </Publication> </PublishedIn> <PublicationDate>2005</PublicationDate> <Authors> <Author> <DisplayName>Biçer, Katherine K. (Katherine Kershen)</DisplayName> <Affiliation> <OrgUnit> </OrgUnit> </Affiliation> </Author> </Authors> <Editors> </Editors> <Publishers> <Publisher> <DisplayName>Massachusetts Institute of Technology</DisplayName> <OrgUnit /> </Publisher> </Publishers> <License>http://dspace.mit.edu/handle/1721.1/7582</License> <Keyword>Materials Science and Engineering.</Keyword> <Abstract>A three phase analytical protocol is developed to systematize the study of multifaceted serpentinite bronze-casting moulds from Bronze Age Anatolia (ca. 3500-1700 B.C.). These moulds represent a class of metal processing tools that reflect material properties and perhaps also social concerns in their development and use. In phase I of the protocol, standard serpentinite tiles are heated to known temperatures and the crack density and ineral changes at each temperature are determined using scanning electron microscopy (SEM) and energy dispersive x-ray (EDX) analysis. These results then serve to calibrate the cracking and mineralogical behaviors of serpentinite replica moulds used in controlled casting experiments during phase II. Metallography on several phase II cast objects provides additional information on heat flow through the stone. In phase III, the protocol is modified appropriately for the non-destructive study of four archaeological moulds using x-ray diffraction (XRD), x-ray fluorescence (XRF), and SEM. The applicability of the protocol to other stone and ceramic materials is discussed.</Abstract> <Access xmlns="http://purl.org/coar/access_right" > </Access> </Publication>