Rapid 3D MAS NMR Spectroscopy at Critical Sensitivity

Author(s)
Matsuki, Yoh; Eddy, Matthew Thomas; Griffin, Robert Guy; Herzfeld, Judith
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Alternative title
Rapid Three-Dimensional MAS NMR Spectroscopy at Critical Sensitivity
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Abstract
Sensitive SIFTing: Multidimensional non-uniform sampling (NUS) NMR spectroscopy is extended to the severely sensitivity-limited regime typical of MAS NMR of biomacromolecules by the use of spectroscopy by the integration of frequency and time domain information (SIFT). A three-dimensional MAS NMR experiment is expedited (here 3.4-fold) without losing sensitivity or resolution.
Date issued
2010-10
URI
http://hdl.handle.net/1721.1/74584
Department
Massachusetts Institute of Technology. Department of Chemistry; Francis Bitter Magnet Laboratory (Massachusetts Institute of Technology)
Journal
Angewandte Chemie International Edition
Publisher
Wiley-Blackwell Pubishers
Citation
Matsuki, Yoh et al. “Rapid Three-Dimensional MAS NMR Spectroscopy at Critical Sensitivity.” Angewandte Chemie International Edition 49.48 (2010): 9215–9218. Web.
Version: Author's final manuscript
ISSN
0570-0833
1521-3773
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